Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. Intergranular corrosion is the proper use, a2622 the specification calls it attack, corrosion is what is taking place.

However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. None of these are identical and cross substitution of results is not possible. Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power xstm and a microsection in any suspicious areas.

A22 level of corrosion is determined by mass loss. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.

ISO is specifically for duplex and all austenitic stainless satm, and recommends ageing at two different temperatures:. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion. As 15 hours is a difficult test period in practice, and is only a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent.

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This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges.


In everyday applications, corrosion varies by materials and solutions. Intergranular simply means that the corrosion a226 taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.

To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or 2a62it is important to understand what causes the process to occur. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.

Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. Link to Active This link will always route to the current Active version of the standard.

Like what you saw? This test should be avoided for most CRAs, except in the circumstances described below, in section 4. Make an Enquiry Notice: Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack.

Intergranular Corrosion Testing: An Overview of ASTM A262

The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. ASTM G28 lists alloys and specifies the test exposure for each. The etch structure types used to atm the specimens are: All austenitic stainless steels should meet this requirement, if proper annealing took place. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.

R Baboian, Corrosion Tests and Standards: Rockwell or Superficial Hardness. The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult. By using our website you consent to all cookies in accordance with our Cookie Policy. A recent publication on intergranular corrosion. Plating and Coating Testing. Some suggested criteria for the listed alloys are shown in Table 2, below.


View more articles about Aerospace Oil and Gas Transportation. We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. Both of these tests should be followed by water quenching.

JavaScript is required for this content. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

ASTM A Testing: An Overview of Intergranular Corrosion | Element

Test Samples Samples may be astk or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long. Based on your materials, application, and requirements, the other 4 methods provide specific focuses. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries.

Discover perspectives, resources, and advice from our world-leading Engaged Experts. ASTM does not give astj warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.

Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.